288-14-2, Isoxazole is a Isoxazoles compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
To the solution of 4a (Ig, 14.5mmol) in trifluoroacetic anhydride (7mL, 50.7mmol) was added ammonium nitrate (1.8g, 22.5mmol) in 0.3g each portion, keeping the reaction temperature between 25-3O0C. After the addition was complete, the mixture was poured into ice water and extracted with DCM (15mLx4). The extract was washed with water and the aqueous layer was extracted with DCM. The combined DCM extract was dried over MgSO4, filtered and concentrated to give a yellow green oil. The oil was triturated by hexane (cooled to 50C) to provide a solid which was filtered to provide 4b (0.72g, 44%).
288-14-2, The synthetic route of 288-14-2 has been constantly updated, and we look forward to future research findings.
Reference£º
Patent; XCOVERY, INC.; WO2009/154769; (2009); A1;,
Isoxazole – Wikipedia
Isoxazole | C3H3NO – PubChem