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Palladium(II) Acetate-Catalyzed Dual C?H Functionalization and C?C Bond Formation: A Domino Reaction for the Synthesis of Functionalized (E)-Bisindole-2-ones from Diarylbut-2-ynediamides
A domino reaction of palladium(II)-catalyzed dual C?H functionalization with subsequent intramolecular annulation is presented. This method provides a convenient synthesis of a range of symmetrical and unsymmetrical biologically important (E)-bisindole-2-ones under extremely mild reaction conditions ? room temperature, green oxidant and no additive. The reaction mechanism is elucidated in light of the yield values as well as additional control experiment results. (Figure presented.).
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Reference£º
Isoxazole – Wikipedia,
Isoxazole | C3H3NO – PubChem