Downstream synthetic route of 32326-25-3

As the paragraph descriping shows that 32326-25-3 is playing an increasingly important role.

32326-25-3, 5-Methoxyisoxazol-3-amine is a Isoxazoles compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated

In a reaction flask equipped with a stirrer, a condenser and a thermometer,4.27 g (0.01 mol) of Intermediate IV-2, 2.00 g (0.02 mol) of potassium bicarbonate,30ml of methanol and 1.14g (0.01mol) 5-methoxy-3-aminoisoxazole, the reaction was refluxed 8h,The reaction was complete by TLC, insolubles were filtered off, the solvent was evaporated and the residue was chromatographed on silica gel,Compound I-5 was obtained as a white solid with a yield of 88% and a purity of 99.7% (HPLC normalization method), 32326-25-3

As the paragraph descriping shows that 32326-25-3 is playing an increasingly important role.

Reference£º
Patent; Tianjin Pharmaceutical Institute; Liu Dengke; Liu Ying; Xie Xiaoshuai; Mu Shuai; Zhang Dashuai; Hou Jiajia; Zou Meixiang; (20 pag.)CN103804367; (2016); B;,
Isoxazole – Wikipedia
Isoxazole | C3H3NO – PubChem