Downstream synthetic route of 36958-61-9

As the paragraph descriping shows that 36958-61-9 is playing an increasingly important role.

36958-61-9, 5-(Bromomethyl)-3-methylisoxazole is a Isoxazoles compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated

A stirred suspension of12(1 g, 3.9 mmol), 5-(bromomethyl)-3-methyl-1,2-oxazole (0.48 mL, 4.3 mmol) and potassium carbonate (1.13 g, 8.2 mmol) in DMF (10 mL) was heated to 80 C for 4 h. After cooling to room temperature the reaction mixture was added to ice-water (100 mL) and stirred for 30 min. The resulting pink precipitate was collected by filtration to afford the title compound (0.89 g, 65%) as a pink powder. 1H NMR (300 MHz, DMSO-d6) delta 8.05-8.00 (m, 2H), 7.94-7.88 (m, 2H), 6.65 (s, 1H), 6.60 (s, 1H), 5.54 (s, 2H), 4.32 (q,J= 7.1 Hz, 2H), 2.25 (s, 3H), 1.31 (t,J= 7.1 Hz, 3H). LC-MS: (High pH) tR1.11 min,m/z351.2 [M-H]-, 96% purity, 36958-61-9

As the paragraph descriping shows that 36958-61-9 is playing an increasingly important role.

Reference£º
Article; Mould, Daniel P.; Bremberg, Ulf; Jordan, Allan M.; Geitmann, Matthis; Maiques-Diaz, Alba; McGonagle, Alison E.; Small, Helen F.; Somervaille, Tim C.P.; Ogilvie, Donald; Bioorganic and Medicinal Chemistry Letters; vol. 27; 14; (2017); p. 3190 – 3195;,
Isoxazole – Wikipedia
Isoxazole | C3H3NO – PubChem