1072-67-9, 5-Methylisoxazol-3-amine is a Isoxazoles compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
2-Chlorosulfonyl-3-methoxy-thiophene (3.8 g, 17.87 MMOL), the product from step A of Preparative Example 13.29, was dissolved in 100 mL of CH2CI2 and 20 mL of pyridine. 3-Amino-5-methyl-isoxazole (3.5 g, 35. 68 MMOL) was added. The mixture was stirred for 20 h at room temperature, diluted with 100 mL of CH2CI2, and washed with a 0.5 N HCI aqueous solution (50 mL x 2), H20 (50 mL), and brine (50 mL). The organic solution was dried with NA2SO4, and conentrated in vacuo to a brown oil. This oil was dissolved in 100 mL of CH2CI2, washed again with a 0.5 M HCI aqueous solution (30 mL x 3) and brine. After dried over NA2SO4, the organic solution was concentrated in vacuo to a yellow solid, 4.48 g (91 %, MH+= 275.0) of the desired product., 1072-67-9
1072-67-9 5-Methylisoxazol-3-amine 66172, aIsoxazoles compound, is more and more widely used in various fields.
Reference£º
Patent; PHARMACOPEIA, INC.; WO2004/33440; (2004); A1;,
Isoxazole – Wikipedia
Isoxazole | C3H3NO – PubChem