Most of the natural products isolated at present are heterocyclic compounds, so heterocyclic compounds occupy an important position in the research of organic chemistry. A compound: 96-13-9, is researched, SMILESS is OCC(Br)CBr, Molecular C3H6Br2OJournal, Organic Chemistry Frontiers called Carbene-catalyzed oxidative acylation promoted by an unprecedented oxidant CCl3CN, Author is Wu, Zijun; Jiang, Di; Wang, Jian, the main research direction is ester preparation; aldehyde alc oxidative acylation carbene catalyst.Quality Control of 2,3-Dibromo-1-propanol.
An unprecedented example of a NHC-catalyzed acylation reaction promoted by an oxidant CCl3CN is described. This protocol features several advantages, including mild reaction conditions, broad substrate scope, and easy operation. In addition, low cost, low b.p., and small mol. weight allow CCl3CN to be an attractive and amenable oxidant. Meanwhile, this formal dehydrogenative coupling reaction of aldehydes RCHO (R = 4-chlorophenyl, quinolin-2-yl, naphthalen-2-yl, etc.) and alcs. R1OH (R1 = Benzyl, 2-methylpiperidin-1-yl, diethylaminyl, etc.) involves a hydride transfer process.
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Reference:
Isoxazole – Wikipedia,
Isoxazole | C3H3NO – PubChem