Product Details of 2402-95-1. The fused heterocycle is formed by combining a benzene ring with a single heterocycle, or two or more single heterocycles. Compound: 2-Chloropyridine 1-oxide, is researched, Molecular C5H4ClNO, CAS is 2402-95-1, about Synthesis of 2-mercaptopyridine-1-oxide zinc salt and its crystal structure. Author is Liu, Rui; Liu, Shan; Zhu, Hongjun.
2-Chloropyridine-N-oxide was synthesized by treating 2-chloropyridine with hydrogen peroxide in glacial acetic acid. The final product 2-mercaptopyridine-1-oxide zinc salt was obtained from 2-chloropyridine-N-oxide via reaction with NaSH, preparation of the sodium salt and chelation with ZnSO4. The structure of the product was characterized by m.p., 1HNMR and single crystal diffractometer. The crystal belonged to monoclinic space group of P21/C with a = 0.84010(17) nm, b = 1.0184(2) nm, c = 1.3736(3) nm, α = 90.00°, β = 97.23(3)°, γ = 90.00°, Dx = 1.810 g/cm3, Z = 4, F(000) = 640, μ = 2.453 mm-1, and the final deviation factor R = (0.0325) and wR = (0.0728).
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Reference:
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